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CAS No 101-61-1 , 4-[[4-(dimethylamino)phenyl]methyl]-N,N-dimethylaniline

  • Name: 4-[[4-(dimethylamino)phenyl]methyl]-N,N-dimethylaniline
  • Synonyms: Methylene base;4-[[4-(dimethylamino)phenyl]methyl]-N,N-dimethylaniline; 101-61-1; Tetrabase; Methane base;Tetra-base; Michler's base; Michler's hydride; 4,4'-Methylenebis(N,N-dimethylaniline);
  • CAS Registry Number:
  • Transport: UN 3077
  • Melting Point: 86-90 ºC
  • Flash Point: 178 ºC
  • Boiling Point: 390 ºC
  • Density: 155
  • Refractive index: 1.615
  • Safety Statements: R45;R50/53
  • Hazard Symbols: N: Dangerous for the environment;T: Toxic;
  • HS Code: 29215990
  • Flash Point: 178 ºC
  • EINECS: 202-959-2
  • Molecular Weight: 254.36998
  • InchiKey: JNRLEMMIVRBKJE-UHFFFAOYSA-N
  • InChI: InChI=1S/C17H22N2/c1-18(2)16-9-5-14(6-10-16)13-15-7-11-17(12-8-15)19(3)
    4/h5-12H,13H2,1-4H3
  • Risk Statements: S45;S53;S60;S61
  • Molecular Formula: C17H22N2
  • Molecular Structure:CAS No:101-61-1 4-[[4-(dimethylamino)phenyl]methyl]-N,N-dimethylaniline

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References of 4-[[4-(dimethylamino)phenyl]methyl]-N,N-dimethylaniline
Title: Michler's Base
CAS Registry Number: 101-61-1
CAS Name: 4,4￠-Methylenebis(N,N-dimethylbenzenamine)
Synonyms: 4,4￠-methylenebis(N,N-dimethylaniline); bis(p-dimethylaminophenyl)methane; 4,4￠-tetramethyldiaminodiphenylmethane; tetra-base; Arnold's base
Molecular Formula: C17H22N2
Molecular Weight: 254.37
Percent Composition: C 80.27%, H 8.72%, N 11.01%
Literature References: Prepd by heating dimethylaniline with 40% formaldehyde and concd HCl: Mekel, DE 1026322 (1958 to BASF); Hey, Sanderson, J. Chem. Soc. 1960, 3203; from dimethylaniline + diacetylperoxide: Horner et al., Ann. 626, 1 (1959); from dimethylaniline + tert-butylperbenzoate: Sosnovsky, Yang, J. Org. Chem. 25, 899 (1960).
Properties: Lustrous leaflets, mp 90-91°. Sublimes without decompn. bp 390°; bp0.1 155-157°. Insol in water. Sol in benzene, ether, carbon disulfide, acids; slightly sol in cold alcohol; more sol in hot alcohol.
Melting point: mp 90-91°
Boiling point: bp 390°; bp0.1 155-157°
CAUTION: This substance is reasonably anticipated to be a human carcinogen: Report on Carcinogens, Eleventh Edition (PB2005-104914, 2004) p III-168.
Use: Has been used in manufacture of dyes. As reagent for lead: Dtsch. Med. Wochenschr. 52, 1855 (1926).