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CAS No 483-64-7 , methyl 3-methoxy-2-(methylamino)benzoate

  • Name: methyl 3-methoxy-2-(methylamino)benzoate
  • Synonyms: 5296-80-0 (hydrochloride); methyl 3-methoxy-2-(methylamino)benzoate; C10588;methyl 3-methoxy-2-(methylamino)benzoate; Nigelline; SureCN2684575; AC1L2I6J; AKOS006292969;483-64-7;
  • CAS Registry Number:
  • Density: 1.143 g/cm3
  • Refractive index: 1.548
  • Molecular Weight: 195.21512
  • InchiKey: ZRWJIZYZTLTXJI-UHFFFAOYSA-N
  • InChI: InChI=1S/C10H13NO3/c1-11-9-7(10(12)14-3)5-4-6-8(9)13-2/h4-6,11H,1-3H3
  • Molecular Formula: C10H13NO3
  • Molecular Structure:CAS No:483-64-7 methyl 3-methoxy-2-(methylamino)benzoate

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483-64-7 3-Methoxy-2-(methylamino)benzoate (Damascenine)

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483-64-7 DAMASCENINE

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References of methyl 3-methoxy-2-(methylamino)benzoate
Title: Damascenine
CAS Registry Number: 483-64-7
CAS Name: 3-Methoxy-2-(methylamino)benzoic acid methyl ester
Synonyms: 2-(methylamino)-m-anisic acid methyl ester; methyl 2-(methylamino)-3-methoxybenzoate; methyldamascenine; nigelline
Molecular Formula: C10H13NO3
Molecular Weight: 195.22
Percent Composition: C 61.52%, H 6.71%, N 7.17%, O 24.59%
Literature References: Odoriferous principle of oil of Nigella from seeds of Nigella damascena L. and Nigella arvensis L., Ranunculaceae. Early syntheses: Ewins, J. Chem. Soc. 101, 544 (1912); Kaufman, Rothlin, Ber. 49, 578 (1916); Sornet, Manuf. Chem. 5, 87 (1924); Keller, Schulze, Arch. Pharm. 263, 481 (1925). Improved synthesis: Mutschler, ibid. 298, 861 (1965); M. Thoinet et al., Ann. Pharm. Fr. 36, 337 (1978). Toxicity study: Bekemeier et al., Arch. Int. Pharmacodyn. Ther. 168, 199 (1967).
Properties: Prisms from abs. alc. Nutmeg-like odor, mp 27-29°. bp 270° (slight dec), bp10 147°. Volatile with steam. Insol in water. Freely sol in alc, ether, chloroform, petr ether, oils.
Melting point: mp 27-29°
Boiling point: bp 270° (slight dec); bp10 147°
 
Derivative Type: Hydrochloride
Properties: Deliquesc prisms, mp 156°. (Hydrate, mp 122°). LD50 orally in mice: 1800 mg/kg (Bekemeier).
Melting point: mp 156°; (Hydrate, mp 122°)
Toxicity data: LD50 orally in mice: 1800 mg/kg (Bekemeier)